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Observation of inter- and intramolecular C---H...F hydrogen bonding in Gingras' salt: [n-Bu4N]+[Ph3SnF2]-

Beckmann, Jens, Dakternieks, Dainis, Duthie, Andrew and Tiekink, Edward R.T. 2002, Observation of inter- and intramolecular C---H...F hydrogen bonding in Gingras' salt: [n-Bu4N]+[Ph3SnF2]-, Journal of organometallic chemistry, vol. 648, no. 1-2, pp. 204-208, doi: 10.1016/S0022-328X(01)01419-X.

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Title Observation of inter- and intramolecular C---H...F hydrogen bonding in Gingras' salt: [n-Bu4N]+[Ph3SnF2]-
Formatted title Observation of inter- and intramolecular C---H...F hydrogen bonding in Gingras' salt: [n-Bu4N]+[Ph3SnF2]-
Author(s) Beckmann, Jens
Dakternieks, Dainis
Duthie, Andrew
Tiekink, Edward R.T.
Journal name Journal of organometallic chemistry
Volume number 648
Issue number 1-2
Start page 204
End page 208
Publisher Elsevier Science B.V.
Place of publication New York, N.Y.
Publication date 2002-04-01
ISSN 0022-328X
1872-8561
Keyword(s) hypercoordination
organotin
fluoride
x-ray structures
119Sn MAS-NMR
Summary The crystal and molecular structure of Gingras' salt [n-Bu4N]+ [Ph3SnF2] is reported, which reveals a variety of inter- and intramolecular C---H...F hydrogen bonding interactions. A 119Sn MAS-NMR spectrum was recorded and a tensor analysis has been performed according to the method of Herzfeld and Berger. The results are discussed in terms of the molecular structure and are compared with the parent compound Ph3SnF as well as with Mes3SnF (Mes=mesityl).


Language eng
DOI 10.1016/S0022-328X(01)01419-X
Field of Research 039904 Organometallic Chemistry
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1 Refereed article in a scholarly journal
Copyright notice ©2002, Elsevier Science B.V.
Persistent URL http://hdl.handle.net/10536/DRO/DU:30001566

Document type: Journal Article
Collection: School of Biological and Chemical Sciences
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