Chemiluminescence detection flow cells for flow injection analysis and high-performance liquid chromatography

Terry, Jessica M., Mohr, Stephan, Fielden, Peter R., Goddard, Nick J., Barnett, Neil W., Olson, Don C., Wolcott, Duane K. and Francis, Paul S. 2012, Chemiluminescence detection flow cells for flow injection analysis and high-performance liquid chromatography, Analytical and bioanalytical chemistry, vol. 403, no. 8, pp. 2353-2360.

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Title Chemiluminescence detection flow cells for flow injection analysis and high-performance liquid chromatography
Author(s) Terry, Jessica M.
Mohr, Stephan
Fielden, Peter R.
Goddard, Nick J.
Barnett, Neil W.
Olson, Don C.
Wolcott, Duane K.
Francis, Paul S.
Journal name Analytical and bioanalytical chemistry
Volume number 403
Issue number 8
Start page 2353
End page 2360
Total pages 8
Publisher Springer
Place of publication Heidelberg, Germany
Publication date 2012-06
ISSN 1618-2642
1618-2650
Keyword(s) acidic potassium permanganate
chemiluminescence
flow cells
high-performance liquid chromatography
Summary We have examined a range of new and previously described flow cells for chemiluminescence detection. The reactions of acidic potassium permanganate with morphine and amoxicillin were used as model systems representing the many fast chemiluminescence reactions between oxidising agents and organic analytes, and the preliminary partial reduction of the reagent was exploited to further increase the rates of reaction. The comparison was then extended to high-performance liquid chromatography separations of α- and β-adrenergic agonists, with permanganate chemiluminescence detection. Flow cells constructed by machining novel channel designs into white polymer materials (sealed with transparent films or plates) have enabled improvements in mixing efficiency and overall transmission of light to the photodetector.
Language eng
Field of Research 030103 Flow Analysis
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1 Refereed article in a scholarly journal
Copyright notice ©2012, Springer-Verlag
Persistent URL http://hdl.handle.net/10536/DRO/DU:30046958

Document type: Journal Article
Collection: School of Life and Environmental Sciences
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