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Preparation and characterization of graphitic carbon nitride through pyrolysis of melamine

Li, Xuefei, Zhang, Jian, Shen, Longhai, Ma, Yanmei, Lei, Weiwei, Cui, Qiliang and Zou, Guangtian 2009, Preparation and characterization of graphitic carbon nitride through pyrolysis of melamine, Applied physics A : materials science and processing, vol. 94, no. 2, pp. 387-392, doi: 10.1007/s00339-008-4816-4.

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Title Preparation and characterization of graphitic carbon nitride through pyrolysis of melamine
Author(s) Li, Xuefei
Zhang, Jian
Shen, Longhai
Ma, Yanmei
Lei, Weiwei
Cui, Qiliang
Zou, Guangtian
Journal name Applied physics A : materials science and processing
Volume number 94
Issue number 2
Start page 387
End page 392
Total pages 6
Publisher Springer
Place of publication Heidelberg, Germany
Publication date 2009-02
ISSN 0947-8396
1432-0630
Keyword(s) anodic oxidation
atomic spectroscopy
auger electron spectroscopy
carbon nitride
chemical bonds
chemical reactions
electron energy loss spectroscopy
Summary Graphitic carbon nitride (g-C3N4) has been synthesized via a two-step pyrolysis of melamine (C3H6N6) at 800°C for 2 h under vacuum conditions. X-ray diffraction (XRD) patterns strongly indicate that the synthesized sample is g-C3N4. Transmission electron microscopy (TEM) and scanning electron microscopy (SEM) morphologies indicate that the product is mainly composed of graphitic carbon nitride. The stoichiometric ratio of C:N is determined to be 0.72 by elemental analysis (EA). Chemical bonding of the sample has been investigated by X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR). Electron energy loss spectroscopy (EELS) verifies the bonding state between carbon and nitrogen atoms. Optical properties of the g-C3N4 were investigated by PL (photoluminescence) measurements and UV–Vis (ultraviolet–visible) absorption spectra. We suppose its luminescent properties may have potential application as component of optical nanoscale devices. Thermogravimetric analysis (TGA) and differential thermal analysis (DTA) were also performed.
Language eng
DOI 10.1007/s00339-008-4816-4
Field of Research 091205 Functional Materials
020504 Photonics, Optoelectronics and Optical Communications
100708 Nanomaterials
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1.1 Refereed article in a scholarly journal
Copyright notice ©2009, Springer-Verlag
Persistent URL http://hdl.handle.net/10536/DRO/DU:30047742

Document type: Journal Article
Collection: Institute for Frontier Materials
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