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Automated methods for the location of the boundaries of chromatographic peaks

Stevenson, Paul G., Gritti, Fabrice and Guiochon, Georges 2011, Automated methods for the location of the boundaries of chromatographic peaks, Journal of chromatography A, vol. 1218, no. 45, pp. 8255-8263, doi: 10.1016/j.chroma.2011.08.088.

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Title Automated methods for the location of the boundaries of chromatographic peaks
Author(s) Stevenson, Paul G.ORCID iD for Stevenson, Paul G.
Gritti, Fabrice
Guiochon, Georges
Journal name Journal of chromatography A
Volume number 1218
Issue number 45
Start page 8255
End page 8263
Total pages 9
Publisher Elsevier BV
Place of publication Amsterdam, The Netherlands
Publication date 2011-11-11
ISSN 0021-9673
Keyword(s) automated data analysis
column efficiency
first peak moment
peak area
peak boundaries
second peak moment
Summary Several simple techniques are presented for the identification of the boundaries of chromatographic peaks. These methods provide a significant reduction in the time needed to perform the rapid, automatic calculation of the central peak moments and to evaluate the quality of a separation while improving the accuracy of the measurements of column efficiencies. It was found that the identification of the peak boundaries as functions of the peak widths and the examination of the slope of the signal to noise versus time plot are viable alternatives to a manual determination.
Language eng
DOI 10.1016/j.chroma.2011.08.088
Field of Research 030108 Separation Science
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1.1 Refereed article in a scholarly journal
Copyright notice ©2011, Elsevier B.V.
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Document type: Journal Article
Collection: School of Life and Environmental Sciences
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Created: Mon, 03 Sep 2012, 14:29:34 EST

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