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Analysis of residues of prometryne and acetochlor in soil-water system by solid-phase extraction and gas chromatography/mass spectrometry

Tan, Wei, Hu, Xiaoxu, Yang, Min, Barrow, Colin J., Yang, Wenrong and Wang, Hongbin 2014, Analysis of residues of prometryne and acetochlor in soil-water system by solid-phase extraction and gas chromatography/mass spectrometry, Desalination and water treatment, vol. 52, no. 4-6, pp. 1177-1182, doi: 10.1080/19443994.2013.827310.

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Title Analysis of residues of prometryne and acetochlor in soil-water system by solid-phase extraction and gas chromatography/mass spectrometry
Author(s) Tan, Wei
Hu, Xiaoxu
Yang, Min
Barrow, Colin J.ORCID iD for Barrow, Colin J. orcid.org/0000-0002-2153-7267
Yang, WenrongORCID iD for Yang, Wenrong orcid.org/0000-0001-8815-1951
Wang, Hongbin
Journal name Desalination and water treatment
Volume number 52
Issue number 4-6
Start page 1177
End page 1182
Total pages 6
Publisher Taylor & Francis
Place of publication Abingdon, England
Publication date 2014
ISSN 1944-3994
1944-3986
Keyword(s) acetochlor
gas chromatography-mass spectrometer
prometryne
soil
solid-phase extraction
Summary A highly sensitive and simple analytical method was developed for analyzing the binary mixed pesticides of prometryne and acetochlor in soil–water system by gas chromatography/mass spectrometry (GC/MS). The sample solution was first purified by C18 solid-phase extraction column, which was leached by acetone. The leachate was enriched to 1.0 mL by pressure blowing concentrator and then analyzed by GC/MS. The linear calibration curves were showed in the range of 1–15 μg/mL with a correlation coefficient of 0.9991. The average recoveries (n = 5) were between 95.3 and 115.7%, with relative standard deviations ranged from 1.71 and 7.95%. The limits of detection of Prometryne/Acetochlor were up to 0.06 and 0.17 μg/mL, respectively. This method provides a reliable approach to examine and evaluate the residues of prometryne and acetochlor in the soil–water system.
Language eng
DOI 10.1080/19443994.2013.827310
Field of Research 030302 Nanochemistry and Supramolecular Chemistry
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1 Refereed article in a scholarly journal
Copyright notice ©2013, Balaban Desalination Publishers
Persistent URL http://hdl.handle.net/10536/DRO/DU:30057772

Document type: Journal Article
Collection: School of Life and Environmental Sciences
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Created: Tue, 12 Nov 2013, 14:54:17 EST

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