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Well-controlled preparation of evenly distributed nanoporous HOPG surface via diazonium salt assisted electrochemical etching process

Cui, Liang, Xu, Yuanhong, Liu, Bingping, Yang, Wenrong, Song, Zhongqian and Liu, Jingquan 2016, Well-controlled preparation of evenly distributed nanoporous HOPG surface via diazonium salt assisted electrochemical etching process, Carbon, vol. 102, pp. 419-425, doi: 10.1016/j.carbon.2016.02.086.

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Title Well-controlled preparation of evenly distributed nanoporous HOPG surface via diazonium salt assisted electrochemical etching process
Author(s) Cui, Liang
Xu, Yuanhong
Liu, Bingping
Yang, WenrongORCID iD for Yang, Wenrong orcid.org/0000-0001-8815-1951
Song, Zhongqian
Liu, Jingquan
Journal name Carbon
Volume number 102
Start page 419
End page 425
Total pages 7
Publisher Elsevier
Place of publication Amsterdam, The Netherlands
Publication date 2016-06-01
ISSN 1873-3891
Summary Evenly distributed nanoporous highly oriented pyrolytic graphite (HOPG) surfaces with controllable pore size were successfully prepared via diazonium salt assisted electrochemical etching method. The porous HOPG was investigated by atomic force microscopy (AFM), Fourier transform infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS) Raman spectroscopy and X-ray diffraction. The size of these pores can be tuned by manipulating the electrochemical etching time. These porous HOPG substrates also demonstrated the enhanced electrocatalytical behaviour and were employed as benign arena for the immobilization of Ru(bpy)32+ for electrochemiluminescence (ECL) sensing applications.
Language eng
DOI 10.1016/j.carbon.2016.02.086
Field of Research 030302 Nanochemistry and Supramolecular Chemistry
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1 Refereed article in a scholarly journal
ERA Research output type C Journal article
Copyright notice ©2016, Elsevier
Persistent URL http://hdl.handle.net/10536/DRO/DU:30085540

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