Influence of hydrogen peroxide in the preparation of nanocrystalline ceria Scholes, F.H., Hughes, A.E., Hardin, S.G., Lynch, P. and Miller, P.R. 2007, Influence of hydrogen peroxide in the preparation of nanocrystalline ceria, Chemistry of materials, vol. 19, no. 9, pp. 2321-2328, doi: 10.1021/cm063024z. Attached Files Name Description MIMEType Size Downloads Title Influence of hydrogen peroxide in the preparation of nanocrystalline ceria Author(s) Scholes, F.H. Hughes, A.E. Hardin, S.G. Lynch, P. orcid.org/0000-0003-3760-4062 Miller, P.R. Journal name Chemistry of materials Volume number 19 Issue number 9 Start page 2321 End page 2328 Total pages 8 Publisher American Chemical Society Place of publication Washington, D.C. Publication date 2007 ISSN 0897-4756 1520-5002 Summary The influence of H2O2 in the preparation of nanocrystalline CeO2 has been investigated by treating solutions of Ce(III) with NaOH in the presence of different concentrations of H2O2. The resulting precipitated material was then examined by a range of techniques, including transmission electron microscopy (TEM), X-ray diffraction (XRD), thermogravimetric analysis (TGA), Raman spectroscopy and X-ray photoelectron spectroscopy (XPS). A decrease in CeO2 crystallite size with increasing H2O2 concentration was observed. This was found to be associated with the formation of an amorphous material containing an η2-peroxide (O22-) species. Language eng DOI 10.1021/cm063024z Field of Research 029999 Physical Sciences not elsewhere classified Socio Economic Objective 970102 Expanding Knowledge in the Physical Sciences HERDC Research category C1.1 Refereed article in a scholarly journal Copyright notice ©2007, American Chemical Society Persistent URL http://hdl.handle.net/10536/DRO/DU:30052455 Document type: Journal Article Collections: Institute for Frontier Materials GTP Research Related Links Link Description Connect to published version (restricted access) Go to link with your DU access privileges     Unless expressly stated otherwise, the copyright for items in DRO is owned by the author, with all rights reserved. Versions Version Filter Type Mon, 13 May 2013, 12:38:38 EST Mon, 13 May 2013, 14:38:02 EST Tue, 14 May 2013, 10:08:11 EST Tue, 18 Jun 2013, 14:21:06 EST Tue, 18 Jun 2013, 14:27:51 EST Fri, 13 Jun 2014, 17:20:59 EST Wed, 27 Aug 2014, 23:30:09 EST Filtered Full Citation counts:   Cited 69 times in TR Web of Science Cited 74 times in Scopus Search Google Scholar Access Statistics: 566 Abstract Views, 0 File Downloads  -  Detailed Statistics Created: Mon, 13 May 2013, 12:38:38 EST