14N overtone magic angle spinning NMR

O'Dell, Luke 2015, 14N overtone magic angle spinning NMR, Annual reports on NMR spectroscopy, vol. 86, pp. 211-236, doi: 10.1016/bs.arnmr.2015.04.003.

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Title 14N overtone magic angle spinning NMR
Formatted title 14N overtone magic angle spinning NMR
Author(s) O'Dell, LukeORCID iD for O'Dell, Luke orcid.org/0000-0002-7760-5417
Journal name Annual reports on NMR spectroscopy
Volume number 86
Start page 211
End page 236
Total pages 26
Publisher Elsevier
Place of publication Amsterdam, The Netherlands
Publication date 2015
ISSN 0066-4103
Keyword(s) 14N solid-state NMR
Dynamic nuclear polarization
Indirect detection
Magic angle spinning
Summary Overtone NMR spectroscopy has the potential to provide high-resolution 14N solid-state NMR spectra. The technique was first developed during the 1980s but has only recently been successfully combined with magic angle spinning (MAS), providing improved sensitivity and resolution as well as enabling more advanced approaches such as indirect detection and signal enhancement methods. This report provides a brief background to 14N overtone NMR, describing the ways in which it differs from conventional NMR and the challenges that arise as a result. The effects of MAS on the overtone spectrum are then presented and illustrated with numerous experimental and simulated examples. Finally, several recent developments enabled by MAS are described and some potential future directions are suggested.
Language eng
DOI 10.1016/bs.arnmr.2015.04.003
Field of Research 020401 Condensed Matter Characterisation Technique Development
Socio Economic Objective 970103 Expanding Knowledge in the Chemical Sciences
HERDC Research category C1 Refereed article in a scholarly journal
ERA Research output type C Journal article
Copyright notice ©2015, Elsevier
Persistent URL http://hdl.handle.net/10536/DRO/DU:30073826

Document type: Journal Article
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